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. 2018 Oct 9;74(Pt 11):1553–1560. doi: 10.1107/S2056989018014020
Rigaku 007HF equipped with Varimax confocal mirrors and an AFC11 goniometer and HyPix 6000 detector diffractometer 1596 independent reflections
Radiation source: Rotating anode, Rigaku 007 HF 1371 reflections with I > 2σ(I)
Detector resolution: 10 pixels mm-1 Rint = 0.095
profile data from ω–scans θmax = 68.2°, θmin = 4.6°
Absorption correction: multi-scan (CrysAlis PRO; Rigaku OD, 2017) h = −5→5
Tmin = 0.507, Tmax = 1.000 k = −15→15
7835 measured reflections l = −17→16