Rigaku 007HF equipped with Varimax confocal mirrors and an AFC11 goniometer and HyPix 6000 detector diffractometer | 1596 independent reflections |
Radiation source: Rotating anode, Rigaku 007 HF | 1371 reflections with I > 2σ(I) |
Detector resolution: 10 pixels mm-1 | Rint = 0.095 |
profile data from ω–scans | θmax = 68.2°, θmin = 4.6° |
Absorption correction: multi-scan (CrysAlis PRO; Rigaku OD, 2017) | h = −5→5 |
Tmin = 0.507, Tmax = 1.000 | k = −15→15 |
7835 measured reflections | l = −17→16 |