| Rigaku FRE+ equipped with VHF Varimax confocal mirrors and an AFC12 goniometer and HyPix 6000 detector diffractometer | 4082 independent reflections |
| Radiation source: Rotating Anode, Rigaku FRE+ | 3761 reflections with I > 2σ(I) |
| Confocal mirrors, VHF Varimax monochromator | Rint = 0.020 |
| Detector resolution: 10 pixels mm-1 | θmax = 27.5°, θmin = 1.9° |
| profile data from ω–scans | h = −9→9 |
| Absorption correction: multi-scan (CrysAlis PRO; Rigaku OD, 2017) | k = −27→27 |
| Tmin = 0.935, Tmax = 1.000 | l = −14→14 |
| 38753 measured reflections |
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