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. 2018 Oct 26;74(Pt 11):1658–1664. doi: 10.1107/S2056989018014895
C1—N1 1.311 (2) C20—C21 1.194 (3)
C1—N2 1.339 (2) C21—C22 1.431 (3)
C1—C2 1.447 (2) C22—C24 1.510 (3)
C2—C3 1.191 (3) C22—C23 1.515 (3)
C3—C4 1.435 (2) C22—H30 1.0000
C4—C5 1.508 (3) C23—C24 1.479 (3)
C4—C6 1.512 (3) C23—H31 0.9900
C4—H2 1.0000 C23—H32 0.9900
C5—C6 1.490 (3) C24—H34 0.9900
C5—H3 0.9900 C24—H33 0.9900
C5—H4 0.9900 C25—N3 1.487 (2)
C6—H5 0.9900 C25—C26 1.522 (2)
C6—H6 0.9900 C25—C30 1.524 (2)
C7—N1 1.483 (2) C25—H35 1.0000
C7—C8 1.517 (2) C26—C27 1.527 (3)
C7—C12 1.523 (2) C26—H37 0.9900
C7—H7 1.0000 C26—H36 0.9900
C8—C9 1.525 (3) C27—C28 1.522 (3)
C8—H8 0.9900 C27—H38 0.9900
C8—H9 0.9900 C27—H39 0.9900
C9—C10 1.520 (3) C28—C29 1.521 (3)
C9—H11 0.9900 C28—H40 0.9900
C9—H10 0.9900 C28—H41 0.9900
C10—C11 1.519 (3) C29—C30 1.528 (3)
C10—H13 0.9900 C29—H43 0.9900
C10—H12 0.9900 C29—H42 0.9900
C11—C12 1.530 (3) C30—H44 0.9900
C11—H15 0.9900 C30—H45 0.9900
C11—H14 0.9900 C31—N4 1.463 (2)
C12—H17 0.9900 C31—C32 1.517 (3)
C12—H16 0.9900 C31—C36 1.526 (3)
C13—N2 1.465 (2) C31—H46 1.0000
C13—C14 1.517 (3) C32—C33 1.531 (3)
C13—C18 1.520 (3) C32—H47 0.9900
C13—H18 1.0000 C32—H48 0.9900
C14—C15 1.529 (3) C33—C34 1.523 (3)
C14—H19 0.9900 C33—H50 0.9900
C14—H20 0.9900 C33—H49 0.9900
C15—C16 1.518 (3) C34—C35 1.519 (3)
C15—H22 0.9900 C34—H52 0.9900
C15—H21 0.9900 C34—H51 0.9900
C16—C17 1.515 (3) C35—C36 1.529 (3)
C16—H24 0.9900 C35—H53 0.9900
C16—H23 0.9900 C35—H54 0.9900
C17—C18 1.530 (3) C36—H56 0.9900
C17—H25 0.9900 C36—H55 0.9900
C17—H26 0.9900 N1—Co 2.0412 (14)
C18—H27 0.9900 N2—H1 0.848 (15)
C18—H28 0.9900 N3—Co 2.0426 (14)
C19—N3 1.311 (2) N4—H29 0.856 (15)
C19—N4 1.344 (2) Co—Cl2 2.2725 (5)
C19—C20 1.445 (2) Co—Cl1 2.2830 (5)
N1—C1—N2 122.55 (16) C24—C22—H30 116.2
N1—C1—C2 121.60 (16) C23—C22—H30 116.2
N2—C1—C2 115.85 (16) C24—C23—C22 60.54 (15)
C3—C2—C1 179.04 (19) C24—C23—H31 117.7
C2—C3—C4 179.4 (2) C22—C23—H31 117.7
C3—C4—C5 119.33 (16) C24—C23—H32 117.7
C3—C4—C6 118.63 (17) C22—C23—H32 117.7
C5—C4—C6 59.10 (13) H31—C23—H32 114.8
C3—C4—H2 116.0 C23—C24—C22 60.89 (16)
C5—C4—H2 116.0 C23—C24—H34 117.7
C6—C4—H2 116.0 C22—C24—H34 117.7
C6—C5—C4 60.58 (13) C23—C24—H33 117.7
C6—C5—H3 117.7 C22—C24—H33 117.7
C4—C5—H3 117.7 H34—C24—H33 114.8
C6—C5—H4 117.7 N3—C25—C26 111.25 (14)
C4—C5—H4 117.7 N3—C25—C30 110.13 (15)
H3—C5—H4 114.8 C26—C25—C30 111.19 (16)
C5—C6—C4 60.33 (13) N3—C25—H35 108.0
C5—C6—H5 117.7 C26—C25—H35 108.0
C4—C6—H5 117.7 C30—C25—H35 108.0
C5—C6—H6 117.7 C25—C26—C27 110.28 (14)
C4—C6—H6 117.7 C25—C26—H37 109.6
H5—C6—H6 114.9 C27—C26—H37 109.6
N1—C7—C8 111.17 (13) C25—C26—H36 109.6
N1—C7—C12 110.67 (14) C27—C26—H36 109.6
C8—C7—C12 110.71 (15) H37—C26—H36 108.1
N1—C7—H7 108.1 C28—C27—C26 111.21 (17)
C8—C7—H7 108.1 C28—C27—H38 109.4
C12—C7—H7 108.1 C26—C27—H38 109.4
C7—C8—C9 110.03 (14) C28—C27—H39 109.4
C7—C8—H8 109.7 C26—C27—H39 109.4
C9—C8—H8 109.7 H38—C27—H39 108.0
C7—C8—H9 109.7 C29—C28—C27 110.56 (19)
C9—C8—H9 109.7 C29—C28—H40 109.5
H8—C8—H9 108.2 C27—C28—H40 109.5
C10—C9—C8 111.47 (17) C29—C28—H41 109.5
C10—C9—H11 109.3 C27—C28—H41 109.5
C8—C9—H11 109.3 H40—C28—H41 108.1
C10—C9—H10 109.3 C28—C29—C30 110.79 (16)
C8—C9—H10 109.3 C28—C29—H43 109.5
H11—C9—H10 108.0 C30—C29—H43 109.5
C11—C10—C9 111.94 (18) C28—C29—H42 109.5
C11—C10—H13 109.2 C30—C29—H42 109.5
C9—C10—H13 109.2 H43—C29—H42 108.1
C11—C10—H12 109.2 C25—C30—C29 111.05 (17)
C9—C10—H12 109.2 C25—C30—H44 109.4
H13—C10—H12 107.9 C29—C30—H44 109.4
C10—C11—C12 111.75 (16) C25—C30—H45 109.4
C10—C11—H15 109.3 C29—C30—H45 109.4
C12—C11—H15 109.3 H44—C30—H45 108.0
C10—C11—H14 109.3 N4—C31—C32 112.41 (14)
C12—C11—H14 109.3 N4—C31—C36 107.71 (15)
H15—C11—H14 107.9 C32—C31—C36 111.12 (16)
C7—C12—C11 111.04 (16) N4—C31—H46 108.5
C7—C12—H17 109.4 C32—C31—H46 108.5
C11—C12—H17 109.4 C36—C31—H46 108.5
C7—C12—H16 109.4 C31—C32—C33 110.59 (15)
C11—C12—H16 109.4 C31—C32—H47 109.5
H17—C12—H16 108.0 C33—C32—H47 109.5
N2—C13—C14 109.88 (15) C31—C32—H48 109.5
N2—C13—C18 111.35 (15) C33—C32—H48 109.5
C14—C13—C18 111.41 (16) H47—C32—H48 108.1
N2—C13—H18 108.0 C34—C33—C32 111.12 (16)
C14—C13—H18 108.0 C34—C33—H50 109.4
C18—C13—H18 108.0 C32—C33—H50 109.4
C13—C14—C15 110.11 (16) C34—C33—H49 109.4
C13—C14—H19 109.6 C32—C33—H49 109.4
C15—C14—H19 109.6 H50—C33—H49 108.0
C13—C14—H20 109.6 C35—C34—C33 110.73 (16)
C15—C14—H20 109.6 C35—C34—H52 109.5
H19—C14—H20 108.2 C33—C34—H52 109.5
C16—C15—C14 111.73 (16) C35—C34—H51 109.5
C16—C15—H22 109.3 C33—C34—H51 109.5
C14—C15—H22 109.3 H52—C34—H51 108.1
C16—C15—H21 109.3 C34—C35—C36 111.74 (16)
C14—C15—H21 109.3 C34—C35—H53 109.3
H22—C15—H21 107.9 C36—C35—H53 109.3
C17—C16—C15 111.59 (16) C34—C35—H54 109.3
C17—C16—H24 109.3 C36—C35—H54 109.3
C15—C16—H24 109.3 H53—C35—H54 107.9
C17—C16—H23 109.3 C31—C36—C35 111.34 (16)
C15—C16—H23 109.3 C31—C36—H56 109.4
H24—C16—H23 108.0 C35—C36—H56 109.4
C16—C17—C18 110.40 (17) C31—C36—H55 109.4
C16—C17—H25 109.6 C35—C36—H55 109.4
C18—C17—H25 109.6 H56—C36—H55 108.0
C16—C17—H26 109.6 C1—N1—C7 116.47 (14)
C18—C17—H26 109.6 C1—N1—Co 125.79 (12)
H25—C17—H26 108.1 C7—N1—Co 117.74 (11)
C13—C18—C17 110.58 (16) C1—N2—C13 124.21 (15)
C13—C18—H27 109.5 C1—N2—H1 117.9 (16)
C17—C18—H27 109.5 C13—N2—H1 116.6 (16)
C13—C18—H28 109.5 C19—N3—C25 116.56 (14)
C17—C18—H28 109.5 C19—N3—Co 125.60 (12)
H27—C18—H28 108.1 C25—N3—Co 117.81 (11)
N3—C19—N4 121.93 (16) C19—N4—C31 126.16 (15)
N3—C19—C20 121.86 (16) C19—N4—H29 117.0 (15)
N4—C19—C20 116.20 (16) C31—N4—H29 116.8 (15)
C21—C20—C19 175.8 (2) N1—Co—N3 111.12 (6)
C20—C21—C22 178.0 (2) N1—Co—Cl2 112.43 (4)
C21—C22—C24 119.2 (2) N3—Co—Cl2 107.90 (4)
C21—C22—C23 118.18 (19) N1—Co—Cl1 107.08 (4)
C24—C22—C23 58.57 (15) N3—Co—Cl1 112.48 (4)
C21—C22—H30 116.2 Cl2—Co—Cl1 105.76 (2)
C3—C4—C5—C6 107.7 (2) C31—C32—C33—C34 57.3 (2)
C3—C4—C6—C5 −108.88 (19) C32—C33—C34—C35 −56.4 (2)
N1—C7—C8—C9 −177.91 (15) C33—C34—C35—C36 55.0 (2)
C12—C7—C8—C9 58.6 (2) N4—C31—C36—C35 178.57 (15)
C7—C8—C9—C10 −57.1 (2) C32—C31—C36—C35 55.0 (2)
C8—C9—C10—C11 54.2 (2) C34—C35—C36—C31 −54.4 (2)
C9—C10—C11—C12 −52.3 (3) N2—C1—N1—C7 173.79 (16)
N1—C7—C12—C11 179.12 (15) C2—C1—N1—C7 −5.4 (2)
C8—C7—C12—C11 −57.1 (2) N2—C1—N1—Co −5.6 (2)
C10—C11—C12—C7 53.7 (2) C2—C1—N1—Co 175.14 (12)
N2—C13—C14—C15 −179.74 (15) C8—C7—N1—C1 150.77 (16)
C18—C13—C14—C15 56.4 (2) C12—C7—N1—C1 −85.76 (19)
C13—C14—C15—C16 −55.0 (2) C8—C7—N1—Co −29.76 (18)
C14—C15—C16—C17 55.4 (2) C12—C7—N1—Co 93.71 (15)
C15—C16—C17—C18 −55.7 (2) N1—C1—N2—C13 167.74 (17)
N2—C13—C18—C17 179.27 (16) C2—C1—N2—C13 −13.0 (3)
C14—C13—C18—C17 −57.7 (2) C14—C13—N2—C1 156.28 (17)
C16—C17—C18—C13 56.6 (2) C18—C13—N2—C1 −79.8 (2)
C21—C22—C23—C24 108.7 (2) N4—C19—N3—C25 176.46 (15)
C21—C22—C24—C23 −107.0 (2) C20—C19—N3—C25 −4.6 (2)
N3—C25—C26—C27 179.25 (16) N4—C19—N3—Co −1.4 (2)
C30—C25—C26—C27 56.1 (2) C20—C19—N3—Co 177.62 (12)
C25—C26—C27—C28 −56.9 (2) C26—C25—N3—C19 149.59 (16)
C26—C27—C28—C29 57.3 (2) C30—C25—N3—C19 −86.66 (19)
C27—C28—C29—C30 −56.5 (3) C26—C25—N3—Co −32.41 (18)
N3—C25—C30—C29 −179.81 (16) C30—C25—N3—Co 91.34 (15)
C26—C25—C30—C29 −56.0 (2) N3—C19—N4—C31 177.89 (16)
C28—C29—C30—C25 56.0 (3) C20—C19—N4—C31 −1.1 (3)
N4—C31—C32—C33 −177.17 (15) C32—C31—N4—C19 −83.8 (2)
C36—C31—C32—C33 −56.4 (2) C36—C31—N4—C19 153.48 (17)