| Stoe IPDS 2T diffractometer | 2495 independent reflections |
| Radiation source: fine-focus sealed tube | 2239 reflections with I > 2σ(I) |
| Detector resolution: 6.67 pixels mm-1 | Rint = 0.037 |
| area detector scans | θmax = 26.0°, θmin = 2.4° |
| Absorption correction: numerical X-Area and X-Red (Stoe & Cie, 2002) | h = −20→21 |
| Tmin = 0.837, Tmax = 0.888 | k = −38→36 |
| 5377 measured reflections | l = −10→12 |
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