| Stoe IPDS 2T diffractometer | 2432 independent reflections |
| Radiation source: fine-focus sealed tube | 2203 reflections with I > 2σ(I) |
| Detector resolution: 6.67 pixels mm-1 | Rint = 0.030 |
| area detector scans | θmax = 26.0°, θmin = 2.4° |
| Absorption correction: numerical X-Area and X-Red (Stoe & Cie, 2002) | h = −21→19 |
| Tmin = 0.851, Tmax = 0.932 | k = −38→36 |
| 5371 measured reflections | l = −10→12 |