| Stoe IPDS 2T diffractometer | 7036 independent reflections |
| Radiation source: fine-focus sealed tube | 6355 reflections with I > 2σ(I) |
| Detector resolution: 6.67 pixels mm-1 | Rint = 0.029 |
| area detector scans | θmax = 26.0°, θmin = 1.9° |
| Absorption correction: numerical X-Area and X-Red (Stoe & Cie, 2002) | h = −17→16 |
| Tmin = 0.838, Tmax = 0.908 | k = −14→15 |
| 18866 measured reflections | l = −25→25 |
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