| Stoe IPDS 2T diffractometer | 7124 independent reflections |
| Radiation source: fine-focus sealed tube | 5922 reflections with I > 2σ(I) |
| Detector resolution: 6.67 pixels mm-1 | Rint = 0.042 |
| area detector scans | θmax = 26.0°, θmin = 2.2° |
| Absorption correction: numerical X-Area and X-Red (Stoe & Cie, 2002) | h = −15→17 |
| Tmin = 0.807, Tmax = 0.938 | k = −15→15 |
| 22018 measured reflections | l = −25→25 |
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