Nonius KapppCCD diffractometer	Rint = 0.068
Detector resolution: 9.4 pixels mm-1	θmax = 24.0°, θmin = 1.1°
phi– and ω–scans	h = −16→16
45373 measured reflections	k = −23→23
18805 independent reflections	l = −47→47
14603 reflections with I > 2σ(I)