Oxford Diffraction Xcalibur E diffractometer | 2232 independent reflections |
Radiation source: fine-focus sealed tube | 2118 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.032 |
ω scans | θmax = 29.8°, θmin = 3.2° |
Absorption correction: analytical [CrysAlis PRO (Agilent, 2014), based on expressions derived by Clark & Reid (1995)] | h = −7→6 |
Tmin = 0.205, Tmax = 0.487 | k = −14→14 |
4320 measured reflections | l = −11→11 |