| Oxford Diffraction Xcalibur E diffractometer | 2288 reflections with I > 2σ(I) |
| Radiation source: sealed tube | Rint = 0.039 |
| ω scans | θmax = 29.9°, θmin = 3.8° |
| Absorption correction: analytical [CrysAlis PRO (Agilent, 2014), based on expressions derived by Clark & Reid (1995)] | h = −7→7 |
| Tmin = 0.286, Tmax = 0.612 | k = −14→14 |
| 5854 measured reflections | l = −11→11 |
| 2458 independent reflections |
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