| Refinement on F2 | Hydrogen site location: mixed |
| Least-squares matrix: full | H-atom parameters constrained |
| R[F2 > 2σ(F2)] = 0.036 | w = 1/[σ2(Fo2) + (0.0603P)2 + 2.7141P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.103 | (Δ/σ)max = 0.001 |
| S = 1.05 | Δρmax = 0.39 e Å−3 |
| 5530 reflections | Δρmin = −0.35 e Å−3 |
| 346 parameters | Extinction correction: SHELXL, Fc*=kFc[1+0.001xFc2λ3/sin(2θ)]-1/4 |
| 26 restraints | Extinction coefficient: 0.0011 (2) |