Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Zn(C48H24N8S4)(C4H10O)]·C4H10O |
| M r | 1054.60 |
| Crystal system, space group | Monoclinic, C2/c |
| Temperature (K) | 200 |
| a, b, c (Å) | 19.8830 (4), 17.1781 (3), 14.8684 (3) |
| β (°) | 91.667 (1) |
| V (Å3) | 5076.18 (17) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.70 |
| Crystal size (mm) | 0.14 × 0.11 × 0.07 |
| Data collection | |
| Diffractometer | Stoe IPDS2 |
| Absorption correction | Numerical (X-RED and X-SHAPE; Stoe, 2008 ▸) |
| T min, T max | 0.807, 0.951 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 39705, 5530, 5042 |
| R int | 0.039 |
| (sin θ/λ)max (Å−1) | 0.639 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.036, 0.103, 1.05 |
| No. of reflections | 5530 |
| No. of parameters | 346 |
| No. of restraints | 26 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.39, −0.35 |