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. 2018 Oct 2;74(Pt 11):1532–1535. doi: 10.1107/S2056989018013610
Oxford Diffraction Gemini diffractometer 5222 independent reflections
Radiation source: sealed X-ray tube 4362 reflections with I > 2σ(I)
Mirror monochromator Rint = 0.060
Detector resolution: 10.4738 pixels mm-1 θmax = 67.3°, θmin = 3.7°
ω scans h = −7→11
Absorption correction: analytical (CrysAlis Pro; Rigaku OD, 2015) k = −25→25
Tmin = 0.216, Tmax = 0.808 l = −17→17
25774 measured reflections