Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [CoCd(C9H10NO2)3Cl2]·H2O |
| M r | 752.78 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 100 |
| a, b, c (Å) | 9.4036 (2), 21.1588 (4), 15.0319 (3) |
| β (°) | 102.221 (2) |
| V (Å3) | 2923.10 (10) |
| Z | 4 |
| Radiation type | Cu Kα |
| μ (mm−1) | 12.38 |
| Crystal size (mm) | 0.29 × 0.07 × 0.02 |
| Data collection | |
| Diffractometer | Oxford Diffraction Gemini |
| Absorption correction | Analytical (CrysAlis PRO; Rigaku OD, 2015 ▸) |
| T min, T max | 0.216, 0.808 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 25774, 5222, 4362 |
| R int | 0.060 |
| (sin θ/λ)max (Å−1) | 0.599 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.046, 0.117, 1.02 |
| No. of reflections | 5222 |
| No. of parameters | 382 |
| No. of restraints | 2 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 2.10, −0.76 |