| Crystal data |
| Chemical formula |
C26H22N2O2
|
|
M
r
|
394.45 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
293 |
|
a, b, c (Å) |
8.654 (5), 10.923 (6), 10.964 (5) |
| α, β, γ (°) |
85.85 (2), 82.38 (2), 74.57 (3) |
|
V (Å3) |
989.4 (9) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.08 |
| Crystal size (mm) |
0.55 × 0.39 × 0.30 |
| |
| Data collection |
| Diffractometer |
Bruker PHOTON 100 CMOS |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2016 ▸) |
|
T
min, T
max
|
0.548, 0.746 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
37627, 4929, 3077 |
|
R
int
|
0.101 |
| (sin θ/λ)max (Å−1) |
0.669 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.069, 0.190, 1.03 |
| No. of reflections |
4929 |
| No. of parameters |
277 |
| No. of restraints |
1 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.72, −0.35 |
