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. 2018 Aug 4;23(8):1947. doi: 10.3390/molecules23081947

Scheme 1.

Scheme 1

Chemical structure of the two fluorophores C1 and C2. The double Knoevenagel condensation between 4-nitrophenylacetic acid or 2-(4-nitrophenyl)acetonitrile respectively and the alkoxy-terephthalaldehyde [22,25] was a convenient symmetric pattern to synthesize the 4,4’-dinitrostilbene skeleton. The identification and purity were assessed by mass spectrometry and 1H-NMR and by comparing melting points with the literature data [22]. The optical properties in solution were analyzed in three solvents with different polarity: dioxane < acetone<DMF (see Table 1).