Table 3.
13C (125 MHz) NMR data of 2–6 in CDCl3
| No. | 2 | 3 | 4 | 5 | 6 |
|---|---|---|---|---|---|
| 1 | 111.7 | 114.5 | 113.1 | 105.8 | 109.2 |
| 2 | 187.8 | 196.9 | 196.0 | 199.9 | 200.2 |
| 3 | 117.4 | 53.0 | 56.4 | 48.1 | 49.3 |
| 4 | 171.4 | 211.8 | 210.4 | 172.3 | 167.4 |
| 5 | 42.5 | 75.0 | 73.7 | 91.0 | 111.9 |
| 6 | 171.6 | 167.5 | 168.6 | 168.5 | 166.6 |
| 7 | 33.0 | 33.9 | 33.7 | 32.8 | 34.0 |
| 8 | 26.3 | 26.1 | 26.6 | 25.6 | 26.2 |
| 9 | 20.4 | 20.5 | 20.5 | 20.4 | 20.6 |
| 10 | 15.3 | 15.5 | 15.7 | 15.4 | 15.9 |
| 11 | 9.6 | 23.8 | 26.7 | 22.7 | 22.2 |
| 12 | 23.6 | 23.9 | 20.6 | 26.4 | 25.8 |
| 13 | 23.6 | 28.3 | 27.8 | 9.9 | |
| 1′ | 86.5 | 89.2 | 88.6 | 87.3 | 89.7 |
| 2′ | 31.5 | 26.1 | 31.3 | 31.7 | 32.0 |
| 3′ | 11.3 | 12.0 | 11.8 | 11.5 | 13.0 |
| 4′ | 32.6 | 34.1 | 33.1 | 32.7 | 34.2 |
| 5′ | 25.1 | 24.3 | 25.2 | 25.2 | 24.8 |
| 6′ | 30.1 | 34.0 | 29.8 | 29.9 | 31.3 |
| 7′ | 30.4 | 30.9 | 30.1 | 29.7 | 28.8 |
| 8′ | 32.3 | 32.6 | 32.3 | 32.4 | 32.5 |
| 9′ | 19.5 | 19.5 | 19.6 | 19.6 | 19.5 |
| 10′ | 19.5 | 19.5 | 19.5 | 19.5 | 20.2 |
| OMe-4 | 61.5 | 55.5 | 61.7 |