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. 2018 Aug 22;23(9):2111. doi: 10.3390/molecules23092111

Table 2.

1H (600 MHz) and 13C-NMR (150 MHz) assignments of compounds 4,5 (CDCl3).

No. 4 5
δ C δH (J in Hz) δ C δH (J in Hz)
1 182.8 179.6
2 143.8 154.8
3 140.4 118.7
4 184.4 185.7
4a 140.0 135.0
5 119.4 7.74, dd, 8.4, 1.2 119.6 7.80, d, 8.4
6 135.0 7.67, t, 8.4 136.2 7.72, t, 8.4
7 117.9 7.29, d, 8.4 117.0 7.27, d, 8.4
8 159.8 160.2
8a 119.8 116.8
1′ 33.2 3.62, s 33.0 2.81, dd, 13.2, 3.6
2.76, dd, 13.2, 7.8
2′ 169.5 67.6 4.12, m
3′ 41.8 3.78, s
4′ 203.1
2′-OCH2CH3 61.4 4.14, m
2′-OCH2CH3 14.1 1.26, t, 6.0
2′-CH3 23.6 1.26, d, 6.6
4′-CH3 30.1 2.30, s
8-OCH3 56.5 4.00, s 56.7 4.04, s