Table 2.
No. | 4 | 5 | ||
---|---|---|---|---|
δ C | δH (J in Hz) | δ C | δH (J in Hz) | |
1 | 182.8 | 179.6 | ||
2 | 143.8 | 154.8 | ||
3 | 140.4 | 118.7 | ||
4 | 184.4 | 185.7 | ||
4a | 140.0 | 135.0 | ||
5 | 119.4 | 7.74, dd, 8.4, 1.2 | 119.6 | 7.80, d, 8.4 |
6 | 135.0 | 7.67, t, 8.4 | 136.2 | 7.72, t, 8.4 |
7 | 117.9 | 7.29, d, 8.4 | 117.0 | 7.27, d, 8.4 |
8 | 159.8 | 160.2 | ||
8a | 119.8 | 116.8 | ||
1′ | 33.2 | 3.62, s | 33.0 | 2.81, dd, 13.2, 3.6 2.76, dd, 13.2, 7.8 |
2′ | 169.5 | 67.6 | 4.12, m | |
3′ | 41.8 | 3.78, s | ||
4′ | 203.1 | |||
2′-OCH2CH3 | 61.4 | 4.14, m | ||
2′-OCH2CH3 | 14.1 | 1.26, t, 6.0 | ||
2′-CH3 | 23.6 | 1.26, d, 6.6 | ||
4′-CH3 | 30.1 | 2.30, s | ||
8-OCH3 | 56.5 | 4.00, s | 56.7 | 4.04, s |