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. 2018 Sep 2;23(9):2232. doi: 10.3390/molecules23092232

Table 1.

Structure, with important hydrogen couplings, and 1H-NMR spectroscopic data (600 MHz) of gibepyrone D and prolipyrone B.

Gibepyrone D (CD3OD) Prolipyrone B (DMSO-d6) graphic file with name molecules-23-02232-i001.jpg
type δH (J in Hz) Type δH (J in Hz)
1 CH3 2.11 (d, 1.3) CH3 2.31 (d, 1.3)
2 CH3 2.36 (d, 1.3) CH2 4.30 (s, brd)
3 CH 6.61 (q, 1.3) CH 6.45 (q, 1.3)
4 CH 6.70 (d, 6.9) CH 6.85 (d, 7.0)
5 CH 7.39 (dq, 1.3; 7.0) CH 7.52 (dt, 1.7; 7.0)