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. Author manuscript; available in PMC: 2018 Nov 13.
Published in final edited form as: Tetrahedron Lett. 2003 Sep 13;44(41):7659–7661. doi: 10.1016/j.tetlet.2003.08.023

Scheme 2. Reagent and conditions:

Scheme 2.

(a) AlMe3, HN(OCH3)-CH3·HCl, CH2Cl2, 23°C, 2.5 h (93%); (b) MEMCl, DIPEA, 23°C, 9 h (92%); (c) iPrMgCl, THF, 23°C, 5 h (61%).