Table 2.
Laboratory | LANL | LLNL | IPGP-CEA |
---|---|---|---|
Instrument | ThermoFisher Neptune MC-ICP-MS |
Nu-Plasma HR MC-ICP-MS |
ThermoFisher Neptune MC-ICP-MS (at IPGP) |
Collectors | 9 Faraday, 7 Channeltron, 1 SEM w/ RPQ |
5 Faraday, 3 SEMs (2 w/ RPQ) |
9 Faraday, 1 SEM w/RPQ |
Introduction System | Stable Signal Spray Chamber | Cetac Aridus II | APEX HF (ESI) |
Nebulizer | PFA-FTST Element Scientific | Cetac PFA Nebulizer | PFA Micro-flow Nebulizer |
Nebulizer Gas Flow | 0.9 L/min | 0.94 L/min | Not Reported |
Solution Uptake | 250 µL/min | 120 µL/min | 50 µL/min |
Mass Bias CRM | CRM U010 (NBL, 2008a) | CRM U010 (NBL, 2008a) | CRM U500 (NBL, 2008b) |
Quality Control CRM | IRMM-035 (IRMM, 1997) CRM 112A (NBL, 2010) |
CRM U005A (NBL, 2008c) | CRM U100 (NBL, 2008d) |
Corrections Applied | Detector Baseline Instrument Background Peak Tailing Detector Gains Mass Bias Hydride Correction |
Detector Baseline Instrument Background Peak Tailing Detector Gains Mass Bias |
Detector Baseline Instrument Background Peak Tailing Detector Gains Mass Bias Hydride Correction |
Summary of instrumental parameters and analysis conditions for thorium isotopic ratio measurements. MC-ICP-MS is Multi-Collector Inductively Coupled Plasma Mass Spectrometry.