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. 2018 Oct 30;14:2730–2736. doi: 10.3762/bjoc.14.251

Table 2.

Photocatalytic conversion of alcohol 1 to bromide 2 in continuous flow.

graphic file with name Beilstein_J_Org_Chem-14-2730-i009.jpg

entry halide source Tres (min) flow rate (μL/min) recovered 1 (%)a yield 2 (%)a yield 3 (%)a

1 NaBr 60 216 89 <5 <5
2 NaBr 120 110 47 53
3 NaBr 240 54.2 45 32 23
4 TBAB 240 110 21 63
5 NaBr 240 110 91(83)b

aYield determined by analysis of 1H NMR. bYield determined by isolation via chromatography.