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. 2008 Mar 4;13(3):567–580. doi: 10.3390/molecules13030567

Table 3.

1H-NMR data (δ, ppm, J, Hz).

graphic file with name molecules-13-00567-i003.jpg
R H4- H7 H8 H10 H11 H13 H14 H17 H18 H19 H20 H21 -NH- -CH3
-OCH3
graphic file with name molecules-13-00567-i004.jpg 7.28- 7.68 m 5.32
s
7.01 d
(7.9)
7.30 d
(7.9)
7.30 d
(7.9)
7.01 d
(7.9)
7.28- 7.68 m 7.28- 7.68 m 7.28- 7.68 m 7.28- 7.68 m 7.28- 7.68 m 11.84 s
12.40 s
-
graphic file with name molecules-13-00567-i005.jpg 7.56- 7.62 m 5.30
s
7.31 d
(8.9)
7.00 d
(9.0)
7.00 d
(9.0)
7.31 d
(8.9)
7.45 d
(8.6)
7.20 d
(8.2)
- 7.20 d
(8.2)
7.45 d
(8.6)
11.79 s
l12.33 sl
2.30 s
graphic file with name molecules-13-00567-i006.jpg 7.45- 7.66 m 5.31
s
7.02 d
(8.9)
7.46 d
(9.0)
7.46 d
(9.0)
7.02 d
(8.9)
7.32 d
(8.8)
6.96 d
(8.8)
- 6.96 d
(8.8)
7.32 d
(8.8)
11.79 s
12.26 s
3.77 s
graphic file with name molecules-13-00567-i007.jpg 7.42- 7.63
m
5.32
s
7.00 d
(9.0)
7.30 d
(9.0)
7.30 d
(9.0)
7.00 d
(9.0)
7.46 d
(8.8)
7.62 d
(8.8)
- 7.62 d
(8.8)
7.46 d
(8.8)
11.90 s
12.38 s
-
graphic file with name molecules-13-00567-i008.jpg 7.42- 7.68 m 5.30
s
6.99 d
(9.1)
7.30 d
(9.1)
7.30 d
(9.1)
6.99 d
(9.1)
- 7.73 d
(2.3)
- 7.81 dd
(8.8; 2.3)
7.96 d
(8.8)
12.12 s
12.43 s
-
graphic file with name molecules-13-00567-i009.jpg 7.40- 7.70m 5.30
s
7.01 d
(8.9)
7.28 d
(8.9)
7.28 d
(8.9)
7.01 d
(8.9)
- 7.40-7.70
m
7.39 dd
(8.9; 2.6)
- 8.11 d
(2.6)
12.16 s
12.53 s
-
graphic file with name molecules-13-00567-i010.jpg 7.42-7.62
m
5.28 s 7.00 d
(8.9)
7.32 d
(8.9)
7.32 d
(8.9)
7.00 d
(8.9)
- 7.54 d
(8.0)
7.37 dd
(8.0; 7.4)
7.54 d
(8.0)
- 11.05 s
11.39 s
-
graphic file with name molecules-13-00567-i011.jpg 7.45- 7.70 m 5.34 s 7.00 d
(8.9)
7.31 d
(8.9)
7.31 d
(8.9)
7.00 d
(8.9)
7.57 s 7.57 s - 7.57 s 7.57 s 11.89 s
12.37 s
-