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. 2008 Feb 7;13(2):340–347. doi: 10.3390/molecules13020340

Table 1.

1,4-Addition of benzylamine to α,β-unsaturated esters.

Entry Product Power (Watts) T (oC) Pressure (psi) Time (min) Yield (%)
1 (±)-3a 37 150 110 180 98
2 (±)-3a 55 140 a 180 83
3 (±)-3b 50 115-130 68 180 97
4 (±)-3b 55 140 a 390 80
5 3c:6 50 115 59 180 50:50b
6 3c:6 50 65 5 10 70:30b
7 3c:6 40 65 c 10 70:30b
8 3c:6 40 65 c 3 90:10b

anot determined.

bRatio between reaction products 3c and 6 (see description results)

cReaction was performed in an open system.