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. 2008 Feb 7;13(2):340–347. doi: 10.3390/molecules13020340

Table 2.

1,4-Addition of (S)-α-methylbenzylamine to α,β-unsaturated esters.

Entry Product Power (Watts) T (oC) Pressure (psi) Time (min) Yield (%)
1 5a 26 150 71 360 74
2 5b 14 130-150 100 540 70
3 5b 48 130-150 a 360 85
4 5c 50 80 18 10 95
5 5c 50 70 b 20 quantitative

a Not determined.

b Reaction was performed in an open system.