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. Author manuscript; available in PMC: 2019 Sep 12.
Published in final edited form as: J Am Chem Soc. 2018 Jul 26;140(36):11317–11324. doi: 10.1021/jacs.8b05868

Table 1.

Sec-alkyl Optimization

graphic file with name nihms-987197-t0007.jpg
a

0.1 mmol scale, yield determined by FID using dodecane as an internal standard.

b

0.3 mmol scale, isolated yield.

c

3 equiv PhSiH3, 6 equiv i-PrOH (anhydrous) instead of Ph(i-PrO)SiH2.