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. Author manuscript; available in PMC: 2019 Sep 12.
Published in final edited form as: J Am Chem Soc. 2018 Jul 26;140(36):11317–11324. doi: 10.1021/jacs.8b05868

Table 2.

Sec-alkyl Olefin Scopea

graphic file with name nihms-987197-t0008.jpg
a

0.3 mmol scale, isolated yield, reaction time: 12—48 h. 1 mL 1,4-dioxane, N2 atmosphere for 2 h, then open to air. All substrates gave >20:1 branched:linear ratio except where notated

b

NMR yield.

c

5 mol% NiBr2(dtbbpy), 800 μL 1,4-dioxane.

d

5 mol% NiBr2(dtbbpy).