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Perpendicular-mode EPR spectra of a 1:1 DMF:THF frozen solution [MnIVH2pout(OH)] at S-band (A) and X-band (B). Sample temperature was 5 K, microwave power was 0.03 mW for S-band and 0.2 mW for X-band. The black traces overlaid on the experimental spectra are the sum of the S = 3/2 simulations for the E/D = 0.17 and 0.33 species in a ratio of 70:30, respectively.
