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. 2009 Jan 9;14(1):298–320. doi: 10.3390/molecules14010298

Table 2.

Methods for the determination of phenolic compounds in solid samples using organic solvents.

Matrix Extraction technique Characteristics Recoveries (%) LOD (µg·g-1) Instrumental Analysis Ref.
Soil Soxhlet Acetone, n-hexane - - GC-MS (SIM) [46]
Soil Soxhlet Methanol 83–97 - LC-UV Vis [64]
Soil MAE Methanol 53–92 0.03–0.08 0.02–0.55 LC-UV andLC-APCI-MS(SIM) [64]
Soil MAE Acetone, n-hexane 32–78 0.010–0.025 GC-MS [61]
Ultrasound agitation 81–99 0.005–0.276 GC-FID [65]
Soil MAE-HS-SPME PA, H2O 86–98 0.0001–0.002 GC-ECD [71]
Soil MAE-SPE C18, acetic anhydride, triethylamine 94–97 0.01–0.2 GC-ECD [72]
Sludge, sediments MAE Methanol, acetone 78–106 0.0001–0.0003 GC-MS/MS [68]
Wood, leather, textiles MAE-SPE C-18, acetic anhydride, triethylamine 100–106 0.01–0.2 GC-ECD [72]