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. 2009 Mar 12;14(3):1126–1133. doi: 10.3390/molecules14031126

Table 2.

Synthesis of quinolines in the presence of H3PW12O40 under solvent-free conditions at 80˚C in 2 hours.

Entry 2-Aminoaryl ketone CH-acid Product Yield (%)a Mp (˚C) Found Mp (˚C) Reported
1 graphic file with name molecules-14-01126-i001.jpg graphic file with name molecules-14-01126-i003.jpg graphic file with name molecules-14-01126-i018.jpg 90 102-103 100-101b
2 graphic file with name molecules-14-01126-i001.jpg graphic file with name molecules-14-01126-i004.jpg graphic file with name molecules-14-01126-i019.jpg 92 110-112 111-112b
3 graphic file with name molecules-14-01126-i001.jpg graphic file with name molecules-14-01126-i005.jpg graphic file with name molecules-14-01126-i020.jpg 94 153-154 156-157c
4 graphic file with name molecules-14-01126-i001.jpg graphic file with name molecules-14-01126-i006.jpg graphic file with name molecules-14-01126-i021.jpg 90 130-131 130-132c
5 graphic file with name molecules-14-01126-i001.jpg graphic file with name molecules-14-01126-i007.jpg graphic file with name molecules-14-01126-i022.jpg 89 192-194 190-192c
6 graphic file with name molecules-14-01126-i001.jpg graphic file with name molecules-14-01126-i008.jpg graphic file with name molecules-14-01126-i023.jpg 92 155-157 155-156c
7 graphic file with name molecules-14-01126-i001.jpg graphic file with name molecules-14-01126-i009.jpg graphic file with name molecules-14-01126-i024.jpg 93 99-100 98-100d
8 graphic file with name molecules-14-01126-i001.jpg graphic file with name molecules-14-01126-i010.jpg graphic file with name molecules-14-01126-i025.jpg 95 152-154 153-154e
9 graphic file with name molecules-14-01126-i001.jpg graphic file with name molecules-14-01126-i011.jpg graphic file with name molecules-14-01126-i026.jpg 94 103-105 105-107f
10 graphic file with name molecules-14-01126-i002.jpg graphic file with name molecules-14-01126-i012.jpg graphic file with name molecules-14-01126-i027.jpg 95 164-166 164-165c
11 graphic file with name molecules-14-01126-i002.jpg graphic file with name molecules-14-01126-i013.jpg graphic file with name molecules-14-01126-i028.jpg 91 150-152 150-151c
12 graphic file with name molecules-14-01126-i002.jpg graphic file with name molecules-14-01126-i014.jpg graphic file with name molecules-14-01126-i029.jpg 89 186-187 185-186c
13 graphic file with name molecules-14-01126-i002.jpg graphic file with name molecules-14-01126-i015.jpg graphic file with name molecules-14-01126-i030.jpg 88 106-108 106-107b
14 graphic file with name molecules-14-01126-i002.jpg graphic file with name molecules-14-01126-i016.jpg graphic file with name molecules-14-01126-i031.jpg 92 207-209 208-209c
15 graphic file with name molecules-14-01126-i002.jpg graphic file with name molecules-14-01126-i017.jpg graphic file with name molecules-14-01126-i032.jpg 94 132-134 133-135b