Table 1.
Polymer | PESu/PPAd Feed | 1H-NMR | [η] (dL/g) | Tm (oC) | -COOH (eq/106g) |
---|---|---|---|---|---|
PESu | 100/0 | 100/0 | 0.28 | 120 | 65 |
P(ESu-co-PAd) 90/10 | 90/10 | 88.9/11.1 | 0.46 | 82 | 54 |
P(ESu-co-PAd) 80/20 | 80/20 | 77.4/22.6 | 0.50 | 60 | 61 |
P(ESu-co-PAd) 70/30 | 70/30 | 67.2/32.8 | 0.43 | 35 | 59 |
P(ESu-co-PAd) 60/40 | 60/40 | 55.6/44.5 | 0.39 | -* | 51 |
P(ESu-co-PAd) 50/50 | 50/50 | 46.7/53.3 | 0.48 | -* | 58 |
P(ESu-co-PAd) 40/60 | 40/60 | 34.4/65.6 | 0.50 | -* | 67 |
P(ESu-co-PAd) 30/70 | 30/70 | 27.3/72.7 | 0.52 | -* | 49 |
P(ESu-co-PAd) 20/80 | 20/80 | 18.7/81.3 | 0.53 | -* | 43 |
P(ESu-co-PAd) 10/90 | 10/90 | 9.1/90.9 | 0.62 | -* | 37 |
PPAd | 0/100 | 0/100 | 0.58 | 43 | 40 |
*amorphous material.