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. 2010 Apr 2;15(4):2398–2404. doi: 10.3390/molecules15042398

Table 1.

NMR data for 3.

Position 1H NMR, δ ppm 13C NMR, δ ppm HMBC
1 164.95
2 6.26 (1H, d, J=13.7 Hz) 120.43 164.95 (C-1) (2J), 142.59(C-3) (2J), 46.96(C-4) (3J)
3 6.82 (1H, m) 142.59 164.95 (C-1) (3J), 120.43 (C-2) (2J), 46.96 (C-4) (2J)
4 3.89 (2H, m) 46.96 120.43 (C-2) (3J), 142.59(C-3) (2J), 169.12(C-5) (2J), 131.05 (C-1’) (3J)
5 169.12
1’ 131.05  
2’ 6.69 (1H, s) 105.36 131.05 (C-1’) (2J), 122.12 (C-6’) (3J)
3’ & 4’ - 147.55  
5’ 6.56 (1H, d, J=8.2 Hz) 108.10 131.05 (C-1’) (3J), 122.12 (C-6’) (2J)
6’ zhzhzzzz 122.12 108.10 (C-5’ )(2J)
OCH2O 6.61 (1H, d, J=2.7 Hz) 100.88 147.55 (C-3’) (3J), 147.55 (C-4’) (3J)
2” 5.86 (2H, s) 43.06 25.54 (C-2”) (2J), 25.54 (C-3”) (3J)
3” & 5” 3.40 (2H, m) 25.54 43.06 (C-1”) (2J), (3J)
4” 1.57 (4H, m) 26.56 25.54 (C-3” ) (2J), 25.54 (C-2”) (3J)
6” 1.57 (2H,m) 46.36 26.56 (C-4”) (2J)
  3.40 (2H, m)