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. 2010 Jun 25;15(7):4589–4598. doi: 10.3390/molecules15074589

Table 2.

13C-NMR data of 1, 2 and 3 (C5D5N, δ ppm)a.

No. 1 2 3 No. 1 2 3
1 37.1 37.0 30.8 Inner Gal-1 102.4 102.3 102.3
2 29.8 29.9 26.8 2 73.1 73.1 81.7
3 75.1 77.5 75.1 3 75.5 75.5 75.1
4 34.7 34.8 30.9 4 80.1 80.2 69.8
5 44.7 44.8 37.0 5 76.1 76.1 76.5
6 28.9 29.0 27.1 6 60.5 60.5 62.1
7 32.2 29.8 26.7 Gal-Glc-1 104.8 104.9 106.0
8 34.3 35.6 35.9 2 81.4 81.4 76.8
9 53.5 47.8 33.7 3 88.4 88.4 78.0
10 35.8 35.5 34.9 4 70.8 70.8 71.7
11 31.6 29.5 29.6 5 77.8 77.8 78.4
12 79.3 71.5 71.7 6 62.3 62.3 62.8
13 46.8 45.6 45.8 3-Glc-1 104.5 104.5
14 55.0 48.3 48.6 2 75.1 75.1
15 32.1 32.5 32.5 3 78.6 78.6
16 81.1 80.9 81.0 4 70.9 70.9
17 63.7 54.5 54.6 5 77.5 77.4
18 11.3 17.4 17.5 6 62.7 62.3
19 12.2 12.2 23.9 2-Glc-1 104.8 104.8
20 41.6 40.9 40.9 2 75.1 75.2
21 15.6 16.2 16.2 3 78.6 78.6
22 110.8 110.6 110.7 4 71.7 71.7
23 37.3 37.2 37.2 5 78.4 78.6
24 28.4 28.4 28.4 6 62.8 62.8
25 34.2 34.2 34.3 C26 Glc-1 105.0 105.0 104.9
26 75.2 75.3 75.3 2 75.2 75.3 75.1
27 17.4 17.4 17.4 3 78.6 78.6 78.3
4 71.5 71.5 71.6
5 78.5 78.4 78.5
6 63.0 63.0 62.8

a Recorded on a Bruker-400 (100 MHz for 13C) NMR spectrometer.