. Author manuscript; available in PMC: 2018 Nov 27.

Published in final edited form as: J Biomol NMR. 2017 Jan 24;67(2):95–108. doi: 10.1007/s10858-016-0086-1

Table 2.

Dephasing rate constants of ¹H magnetization for different types of ¹³C and ¹⁵N spins in U-¹³C,¹⁵N-LC8, U-¹³C,¹⁵N-CAP-Gly and U-¹³C,¹⁵N-CAP-Gly/n.a. EB1 complex

U-¹³C,¹⁵N-LC8

Peak regions	Inverse time constant 1/τ (coefficient values ± standard deviation) (s⁻¹) ^a
	N-H REDOR	C-H REDOR	dREDOR	dREDORsatC
¹³C’	9.6 ± 1.9	5.3 ± 2.2	10.8 ± 5.0	9.4 ± 1.7
¹³Cα	0.2 ± 0.6	9.8 ± 2.2	11.3 ± 3.5	6.9 ± 1.1
Aromatic ¹³C		17.5 ± 1.4	25.3 ± 6.2
Sidechains ¹³C	0.2 ± 0.1	8.3 ± 1.6	8.9 ± 2.0	6.2 ± 0.6
Backbone ¹⁵N	17.8 ± 6.6		22.1 ± 4.3

U-¹³C,¹⁵N-CAP-Gly

Peak regions	Inverse time constant 1/τ (coefficient values ± standard deviation) (s⁻¹)			y₀
	N-H REDOR	C-H REDOR	dREDOR	dREDOR
¹³C’		6.8 ± 0.3	11.3 ± 1.9
¹³Cα		7.8 ± 1.2	7.5 ± 2.2	−0.1 ± 0.1
Sidechains ¹³C		8.2 ± 0.8	8.7 ± 1.4

U-¹³C,¹⁵N-CAP-Gly/EB1

Peak regions	Inverse time constant 1/τ (coefficient values ± standard deviation) (s⁻¹)			y₀
	N-H REDOR	C-H REDOR	dREDOR	dREDOR
¹³Cα			5.9 ± 2.0	0.4 ± 0.0

Dephasing curves are fitted to exponential decay function: y = y₀+ Aexp(−x /τ ) τ is the time constant.