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. 2010 Nov 16;15(11):8400–8424. doi: 10.3390/molecules15118400

Table 9.

Yield of water mediated N-Boc-aniline deprotection at different temperatures [77].

Entry Temperature (°C) Time (h) Isolated yield (%)
1 30 4 0
2 80 4 0
3 130 2 12
4 130 4 39
5 150 2 38
6 150 4 86