Table 1.
No. | δ c | δ H | HMBC (H to C) |
---|---|---|---|
1 | 165.4 | – | – |
2 | – | – | – |
3 | 45.3 | 3.51 (m) | C-1, 4, −5, −6 |
3.61 (m) | C-1, 4, −5, −6 | ||
4 | 22.6 | 2.00 (m) | C-3, −5, −6 |
2.06 (m) | C-3, −5, −6 | ||
5 | 28.1 | 2.34 (m) | C-4, −6, −7 |
C-4, −6, −7 | |||
6 | 59.0 | 4.11 (t, 7.5) | C-4, −5, −7 |
7 | 170.2 | – | – |
8 | – | 6.73 (s) | – |
9 | 65.6 | 4.36 (dt, 6.5, 3.0) | C-7, −11 |
10 | 59.4 | 3.97 (d, 3.0) | C-1, −9, −11 |
11 | 18.9 | 1.34 (d, 6.5) | C-9, −10 |
12 | – | 1.89 (m) | – |