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. 2010 Feb 10;15(2):871–877. doi: 10.3390/molecules15020871

Table 1.

1H- (500 MHz) and 13C-NMR (125 MHz) data of compound 1 (in CDCl3, δ in ppm, J in Hz).

No. δ c δ H HMBC (H to C)
1 165.4
2
3 45.3 3.51 (m) C-1, 4, −5, −6
3.61 (m) C-1, 4, −5, −6
4 22.6 2.00 (m) C-3, −5, −6
2.06 (m) C-3, −5, −6
5 28.1 2.34 (m) C-4, −6, −7
C-4, −6, −7
6 59.0 4.11 (t, 7.5) C-4, −5, −7
7 170.2
8 6.73 (s)
9 65.6 4.36 (dt, 6.5, 3.0) C-7, −11
10 59.4 3.97 (d, 3.0) C-1, −9, −11
11 18.9 1.34 (d, 6.5) C-9, −10
12 1.89 (m)