Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.
Reaction between o-phenylene diamine and phenylglyoxal monohydrate in the presence of iodine (5 mol%) in different solvents under microwave irradiation.
 |
| Entry | Solvent | Time (min.) | Yield (%) |
|---|---|---|---|
| 1 | Methanol | 3 | 41 |
| 2 | Ethanol | 3 | 65 |
| 3 | Tetrahydrofuran | 5 | 48 |
| 4 | Dichloromethane | 3 | 27 |
| 5 | THF/Water (1:1) | 5 | 36 |
| 6 | Water | 5 | 38 |
| 7 | Acetonitrile | 3 | 72 |
| 8 | Ethanol/Water (1:1) | 30 sec. | 99 |
