Table 1.
No. | A | B | C | D | Pressure | Temperature | Time | Flow | Extraction |
---|---|---|---|---|---|---|---|---|---|
Pressure | Temperature | Time | Flow rate | MPa | °C | min | rate L/h | yield (%) | |
1 | 0 | 0 | 0 | 0 | 25 | 60 | 90 | 25 | 29.92 |
2 | 1 | −1 | 1 | 1 | 30 | 50 | 120 | 30 | 32.58 |
3 | 1 | −1 | 1 | −1 | 30 | 50 | 120 | 20 | 31.17 |
4 | 1 | −1 | −1 | 1 | 30 | 50 | 60 | 30 | 29.47 |
5 | 0 | 0 | 0 | −2 | 25 | 60 | 90 | 15 | 28.09 |
6 | 1 | 1 | −1 | 1 | 30 | 70 | 60 | 30 | 30.53 |
7 | 1 | 1 | 1 | −1 | 30 | 70 | 120 | 20 | 34.42 |
8 | −1 | −1 | −1 | −1 | 20 | 50 | 60 | 20 | 25.01 |
9 | −1 | 1 | −1 | −1 | 20 | 50 | 60 | 20 | 15.21 |
10 | 0 | −2 | 0 | 0 | 25 | 60 | 60 | 30 | 30.11 |
11 | −1 | −1 | 1 | −1 | 20 | 50 | 90 | 20 | 28 |
12 | 0 | 0 | −2 | 0 | 25 | 60 | 30 | 25 | 25.13 |
13 | 0 | 0 | 0 | 0 | 25 | 60 | 90 | 25 | 31.97 |
14 | 0 | 0 | 0 | 0 | 25 | 60 | 90 | 25 | 33.06 |
15 | 0 | 0 | 0 | 0 | 25 | 60 | 90 | 25 | 29.52 |
16 | −1 | 1 | 1 | −1 | 20 | 70 | 120 | 20 | 27.07 |
17 | −1 | 1 | 1 | 1 | 20 | 70 | 120 | 30 | 27.54 |
18 | −1 | −1 | −1 | 1 | 20 | 50 | 60 | 30 | 28.33 |
19 | 2 | 0 | 0 | 0 | 35 | 60 | 90 | 25 | 30.32 |
20 | 0 | 0 | 0 | 0 | 20 | 60 | 90 | 25 | 33.05 |
21 | −2 | 0 | 0 | 0 | 15 | 60 | 90 | 25 | 11.79 |
22 | 1 | 1 | 1 | 1 | 30 | 70 | 120 | 30 | 35.56 |
23 | −1 | 1 | −1 | 1 | 20 | 70 | 60 | 30 | 17.44 |
24 | 0 | 0 | 0 | 2 | 25 | 60 | 90 | 35 | 30.66 |
25 | 0 | 2 | 0 | 0 | 25 | 80 | 90 | 25 | 31.82 |
26 | 0 | 0 | 2 | 0 | 25 | 60 | 150 | 25 | 30.18 |
27 | 1 | −1 | −1 | −1 | 30 | 50 | 60 | 20 | 31.06 |
28 | 0 | 0 | 0 | 0 | 25 | 60 | 90 | 25 | 31.98 |
29 | 1 | 1 | −1 | −1 | 30 | 70 | 60 | 20 | 30.73 |
30 | −1 | −1 | 1 | 1 | 20 | 50 | 120 | 30 | 28.15 |