1 |
|
129.8 |
|
|
131.4 |
2 |
6.78 (1H,
d, J = 1.2 Hz) |
115.1 |
|
6.59 (1H,
d, J = 1.6 Hz) |
117.0 |
3 |
|
146.3 |
|
|
146.0 |
4 |
|
146.6 |
|
|
144.6 |
5 |
6.69 (1H,
d, J = 8.2 Hz) |
116.4 |
|
6.57 (1H,
d, J = 8.0 Hz) |
116.3 |
6 |
6.66 (1H,
dd, J = 8.2, 1.2 Hz) |
119.5 |
|
6.48 (1H,
dd, J = 8.0, 1.6 Hz) |
121.4 |
7 |
4.50 (1H,
dd, J = 10.2, 2.8 Hz) |
78.7 |
|
2.67 (2H,
t, J = 7.2 Hz) |
36.7 |
8 |
3.90 (1H,
dd, J = 12.0, 2.8 Hz) |
72.6 |
|
3.94 (1H,
m) |
72.0 |
|
3.61 (1H,
dd, J = 12.0, 10.2 Hz) |
|
|
3.63 (1H,
m) |
|
1′ |
|
127.8 |
|
|
127.8 |
2′ |
7.01 (1H,
d, J = 2.0 Hz) |
115.5 |
|
7.06 (1H,
d, J = 1.2 Hz) |
115.2 |
3′ |
|
146.9 |
|
|
146.8 |
4′ |
|
149.8 |
|
|
149.6 |
5′ |
6.73 (1H,
d, J = 8.2 Hz) |
116.5 |
|
6.77 (1H,
d, J = 8.4 Hz) |
116.5 |
6′ |
6.91 (1H,
dd, J = 8.2, 2.0 Hz) |
123.1 |
|
6.91 (1H,
dd, J = 8.4, 1.2 Hz) |
123.0 |
7′ |
6.25 (1H,
d, J = 16.0 Hz) |
147.8 |
|
6.27 (1H,
d, J = 16.0 Hz) |
147.1 |
8′ |
7.55 (1H,
d, J = 16.0 Hz) |
114.6 |
|
7.56 (1H,
d, J = 16.0 Hz) |
115.2 |
9′ |
|
168.2 |
|
|
168.4 |
1′′ |
4.51 (1H,
d, J = 7.6 Hz) |
99.9 |
|
4.49 (1H,
d, J = 8.0 Hz) |
102.4 |
2′′ |
3.40 (1H,
m) |
74.3 |
|
4.80 (1H,
t, J = 8.0 Hz) |
75.1 |
3′′ |
5.25 (1H,
t, J = 8.8 Hz) |
76.0 |
|
3.56 (1H,
t, J = 8.8 Hz) |
76.2 |
4′′ |
3.62 (1H,
m) |
70.2 |
|
3.38 (1H,
m) |
71.7 |
5′′ |
3.67 (1H,
m) |
78.5 |
|
3.44 (1H,
m) |
76.9 |
6′′ |
3.45 (1H,
dd, J = 11.2, 5.2 Hz) |
67.8 |
|
3.65 (1H,
dd, J = 10.8, 5.0 Hz) |
67.9 |
|
3.72 (1H,
dd, J = 11.2, 1.7 Hz) |
|
|
4.00 (1H,
dd, J = 10.8, 1.2 Hz) |
|
1′′′ |
4.73 (1H,
d, J = 0.8 Hz) |
102.3 |
|
4.74 (1H,
d, J = 1.6 Hz) |
102.2 |
2′′′ |
3.85 (1H,
m) |
72.0 |
|
3.84 (1H,
m) |
72.3 |
3′′′ |
3.70 (1H,
m) |
72.4 |
|
3.70 (1H,
m) |
72.2 |
4′′′ |
3.37 (1H,
m) |
74.0 |
|
3.37 (1H,
m) |
74.0 |
5′′′ |
3.71 (1H,
m) |
69.9 |
|
3.70 (1H,
m) |
69.8 |
6′′′ |
1.26 (1H,
d, J = 6.5 Hz) |
18.0 |
|
1.26 (1H,
d, J = 6.0 Hz) |
18.1 |