Table 9.
Transformation | Time [min] | Dwell device | Batch |
---|---|---|---|
Yields/Conv. [%] a | Yields/Conv. [%] a | ||
28 → 29 | 3.4 | 5 | 2 |
11 | 23 | 7 | |
21 | 44 | 19 | |
40 | 74 | 39 | |
60 | 92 | 59 (22 b) | |
30a → 31a | 21 | 33 | 46 |
40 | 69 | 53 | |
60 | 77 | 69 (19 b) | |
30b → 31b | 21 | 39 | 36 |
40 | 70 | 59 | |
60 | 80 | 72 (21 b) | |
29 + 32a → 33a | 14 | 83 | 46 |
21 | 97 | 93 | |
40 | 100 | 100 | |
60 | 100 | 100 (29 b) | |
29 + 32b → 33b | 14 | 4 | 2 |
21 | 34 | 20 | |
40 | 66 | 44 | |
60 | 100 | 86 (17 b) |
a Conversions for reactions 28 →29 and 29 + 32 → 33. Yields for reactions 30 → 31; b Batch reactor with 5 × 8 W lamps.