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Key parameters of batch vs. microreactor used.
| Batch | μ-Reactor |
|---|---|
| Cylindrical glass vessel 75 × 300 mm (ID × H) 600 g (msolution) | FEP tube (wrapped around a quartz beaker) 0.5–1.6 mm × 6.4–19.2 m (ID × L) 0.8–12.9 mL (Vcapillary) |
| 400 W high pressure mercury lamp (inside a Pyrex immersion well; immersed in glass vessel) | 400 W high pressure mercury lamp (inside a Pyrex immersion well; placed inside the quartz beaker) |
