Table 3.
Refinement statistics for crystal structure data collection of the lectin from the seeds of Dioclea wilsonii (DwL).
| Data Collection * | |
|---|---|
| Point group | I222 |
| Unit cell parameters (Å) | |
| A | 59.6 |
| B | 67.9 |
| C | 109.0 |
| Unit cell angles (°) | |
| α = β = γ | 90 |
| Total number of reflection | 50274 (6863) |
| Total number of unique observations | 10483 (1526) |
| Resolution limit (Å) | 23.29–2.2 |
| Rmerge (%) a | 8.4 (24.1) |
| Completeness (%) | 97.1 (98.5) |
| Multiplicity (%) | 4.8 (4.5) |
| (I)/σ | 5.0 (1.8) |
| Matthews coefficient (Å3.Da−1) | 2.17 |
| Solvent content (%) | 43.28 |
| Wavelenght (Å) | 1.42 |
* Values in parenthesis represent the high resolution shell; a
where I(hkl)i is the intensity of ith measurement of the reflection h and I(hkl) is the mean value of the I(hkl)i for all I measurements.