Table 1.
Position | 13C-NMR a | 1H-NMR b |
---|---|---|
1 | n.d. c | |
2 | 120.1 | 5.97 (1H, d, J = 15.5) |
3 | 146.9 | 7.10 (1H, d, J = 15.5) |
4 | 134.3 | |
5 | 141.1 | 5.86 (1H, d, J = 9.5) |
6 | 41.6 | 4.48 (1H, m) |
7 | 201.4 | |
8 | 124.6 | |
9,13 | 131.8 | 7.81 (2H, d, J = 9.0) |
10,12 | 111.9 | 6.67 (2H,d, J = 9.0) |
11 | 155.4 | |
4-Me | 12.7 | 1.80 (3H, s) |
6-Me | 18.2 | 1.22 (3H, d, J = 6.5) |
N-Me2 | 40.2 | 3.02 (6H, s) |
a: 500MHz in CD3OD; b: 500MHz in CD3OD; c: Not detected.