Table 2.
Optimization of different extraction conditions.
| Condition | Parameter | Recovery | |||||
|---|---|---|---|---|---|---|---|
| 3AcDON/15AcDON | T-2 | F-X | NIV | DON | ZEA | ||
| Formic Acid (%) |
0.5 | 82% | 95% | 78% | 79% | 9% | 91% |
| 1 | 91% | 90% | 91% | 77% | 94% | 96% | |
| 1.5 | 90% | 72% | 80% | 79% | 90% | 95% | |
| 2 | 91% | 99% | 86% | 72% | 74% | 77% | |
| Sonication (min) |
1 | 89% | 75% | 80% | 82% | 63% | 74% |
| 2 | 95% | 91% | 90% | 94% | 101% | 81% | |
| 3 | 95% | 75% | 92% | 82% | 101% | 86% | |
| 4 | 100% | 90% | 91% | 81% | 99% | 88% | |
| Extract Volume (mL) |
10 | 91% | 80% | 90% | 68% | 80% | 93% |
| 15 | 98% | 102% | 80% | 70% | 84% | 77% | |
| 20 | 102% | 99% | 94% | 84% | 90% | 91% | |
| 25 | 95% | 101% | 96% | 69% | 95% | 90% | |