Appendix A-3.
Contents of moisture and analytes in Danshen during drying at100, 110 and 120 °C (n = 3).
| Temp. | Analytes | Drying time (min) | ||||||
|---|---|---|---|---|---|---|---|---|
| 0 | 20 | 40 | 60 | 80 | 100 | 120 | ||
| 100 °C | Moisture (%) | 70.10 ± 0.15 | 65.37 ± 0.14 | 57.56 ± 0.65 | 47.63 ± 1.03 | 33.15 ± 1.55 | 16.77 ± 1.15 | 7.16 ± 0.41 |
| Sa B (mg/g) | 0.79 ± 0.03 | 0.96 ± 0.04 | 1.24 ± 0.11 | 4.35 ± 0.72 | 36.03 ± 2.72 | 34.34 ± 1.33 | 27.66 ± 1.53 | |
| dTN (mg/g) | 0.18 ± 0.02 | 0.20 ± 0.01 | 0.27 ± 0.02 | 0.30 ± 0.01 | 0.26 ± 0.00 | 0.18 ± 0.01 | 0.15 ± 0.02 | |
| cTN (mg/g) | 1.17 ± 0.15 | 1.25 ± 0.05 | 1.71 ± 0.10 | 2.16 ± 0.05 | 1.74 ± 0.02 | 1.1 ± 0.05 | 0.9 ± 0.08 | |
| TN I (mg/g) | 1.39 ± 0.11 | 1.44 ± 0.12 | 1.84 ± 0.14 | 2.42 ± 0.13 | 1.85 ± 0.09 | 1.28 ± 0.11 | 1.00 ± 0.12 | |
| TN IIA (mg/g) | 3.77 ± 0.38 | 3.81 ± 0.23 | 5.03 ± 0.32 | 6.23 ± 0.33 | 5.01 ± 0.26 | 3.20 ± 0.28 | 2.47 ± 0.27 | |
| TTNs (mg/g) | 6.51 ± 0.22 | 6.70 ± 0.08 | 8.85 ± 0.17 | 11.11 ± 0.11 | 8.86 ± 0.05 | 5.76 ± 0.10 | 4.52 ± 0.14 | |
| 110 °C | Moisture (%) | 70.10 ± 0.15 | 62.69 ± 0.65 | 49.42 ± 2.14 | 31.81 ± 4.03 | 12.92 ± 2.46 | 4.40 ± 0.42 | 1.47 ± 0.22 |
| Sa B (mg/g) | 0.79 ± 0.03 | 0.84 ± 0.02 | 1.04 ± 0.16 | 38.10 ± 1.34 | 36.21 ± 1.46 | 31.62 ± 0.70 | 28.95 ± 1.01 | |
| dTN (mg/g) | 0.18 ± 0.02 | 0.20 ± 0.01 | 0.21 ± 0.02 | 0.24 ± 0.01 | 0.18 ± 0.00 | 0.17 ± 0.00 | 0.13 ± 0.00 | |
| cTN (mg/g) | 1.17 ± 0.15 | 1.45 ± 0.04 | 1.53 ± 0.01 | 1.62 ± 0.03 | 1.16 ± 0.03 | 1.05 ± 0.01 | 0.73 ± 0.02 | |
| TN I (mg/g) | 1.39 ± 0.11 | 1.44 ± 0.12 | 1.46 ± 0.14 | 1.98 ± 0.06 | 1.58 ± 0.05 | 1.44 ± 0.05 | 0.98 ± 0.06 | |
| TN IIA (mg/g) | 3.77 ± 0.38 | 4.53 ± 0.22 | 4.89 ± 0.31 | 5.04 ± 0.10 | 3.66 ± 0.08 | 3.36 ± 0.02 | 2.07 ± 0.07 | |
| TTNs (mg/g) | 6.51 ± 0.22 | 7.62 ± 0.08 | 8.09 ± 0.19 | 8.88 ± 0.05 | 6.58 ± 0.05 | 6.02 ± 0.02 | 3.91 ± 0.03 | |
| 120 °C | Moisture (%) | 70.10 ± 0.15 | 60.13 ± 0.66 | 45.36 ± 1.90 | 26.74 ± 2.37 | 11.32 ± 0.25 | 3.74 ± 0.19 | 2.12 ± 0.25 |
| Sa B (mg/g) | 0.79 ± 0.03 | 1.34 ± 0.08 | 24.3 ± 2.15 | 36.2 ± 1.30 | 40.03 ± 0.78 | 37.5 ± 0.94 | 36.42 ± 1.59 | |
| dTN (mg/g) | 0.18 ± 0.02 | 0.20 ± 0.01 | 0.25 ± 0.00 | 0.21 ± 0.01 | 0.22 ± 0.01 | 0.20 ± 0.01 | 0.19 ± 0.01 | |
| cTN (mg/g) | 1.17 ± 0.15 | 1.33 ± 0.04 | 1.56 ± 0.03 | 1.43 ± 0.06 | 1.23 ± 0.02 | 1.01 ± 0.08 | 0.85 ± 0.03 | |
| TN I (mg/g) | 1.39 ± 0.11 | 1.51 ± 0.09 | 1.91 ± 0.08 | 1.85 ± 0.20 | 1.83 ± 0.02 | 1.62 ± 0.15 | 1.49 ± 0.11 | |
| TN IIA (mg/g) | 3.77 ± 0.38 | 4.35 ± 0.21 | 4.84 ± 0.19 | 4.13 ± 0.32 | 3.62 ± 0.09 | 2.88 ± 0.25 | 2.65 ± 0.38 | |
| TTNs (mg/g) | 6.51 ± 0.22 | 7.39 ± 0.08 | 8.56 ± 0.06 | 7.62 ± 0.12 | 6.90 ± 0.13 | 5.71 ± 0.13 | 5.18 ± 0.09 | |