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. 2012 May 25;17(6):6395–6414. doi: 10.3390/molecules17066395

Table 6.

Isolated yields of indolino[60]fullerene derivatives.

Entry Aromatic Amine 5- N- Yield / % a
8a 4-Dodecylaniline n-C12H25 H 77.7
8b 4- n-Butylaniline n-C4H9 H 64.1
8c p-Toluidine Me H 84.0
8d 4-Fluoroaniline F H 75.7
8e Aniline H H 78.9
8f N-Me-p-toluidine Me Me 29.3

a Isolated yield, estimated from HPLC areas. Reaction conditions: C60O 100 mg, 0.136 mmol; aromatic amines 1.357 mmol; Sepiolite 2.0 g; chlorobenzene 100 mL, 100 °C.