Table 1.
Selected bond lengths [Ǻ] and Selected bond angles [°] for compounds 8 and 9.
| 8 | 9 | ||||||
|---|---|---|---|---|---|---|---|
| Zn1 | Br1 | 2.4036(4) | Zn1 | N1 | 2.1752(18) | ||
| Zn1 | Br2 | 2.4172(4) | Zn1 | N2 | 2.0752(18) | ||
| Zn1 | N1 | 2.243(3) | Zn1 | N3 | 2.217(2) | ||
| Zn1 | N2 | 2.076(2) | Zn1 | N4 | 1.9681(18) | ||
| Zn1 | N3 | 2.331(2) | Zn1 | N5 | 1.9698(19) | ||
| Br1 | Zn1 | Br2 | 116.905(15) | N1 | Zn1 | N3 | 154.18(7) |
| N1 | Zn1 | Br1 | 92.48(6) | N2 | Zn1 | N1 | 75.30(7) |
| N1 | Zn1 | Br2 | 95.00(6) | N2 | Zn1 | N3 | 79.64(8) |
| N1 | Zn1 | N3 | 151.50(8) | N4 | Zn1 | N1 | 97.48(7) |
| N2 | Zn1 | Br1 | 133.79(6) | N4 | Zn1 | N2 | 133.47(8) |
| N2 | Zn1 | Br2 | 108.28(6) | N4 | Zn1 | N3 | 95.22(7) |
| N2 | Zn1 | N1 | 73.92(9) | N4 | Zn1 | N5 | 113.13(8) |
| N2 | Zn1 | N3 | 79.37(9) | N5 | Zn1 | N1 | 96.56(7) |
| N3 | Zn1 | Br1 | 99.01(6) | N5 | Zn1 | N2 | 113.35(8) |
| N3 | Zn1 | Br2 | 102.71(5) | N5 | Zn1 | N3 | 98.97(8) |
| C1 | N1 | Zn1 | 128.0(2) | C1 | N1 | Zn1 | 126.71(14) |
| C5 | N1 | Zn1 | 113.25(18) | C5 | N1 | Zn1 | 114.26(14) |
| C6 | N2 | Zn1 | 120.85(19) | C6 | N2 | Zn1 | 120.19(15) |
| C8 | N2 | Zn1 | 115.86(19) | C8 | N2 | Zn1 | 114.51(17) |
| C9 | N3 | Zn1 | 100.28(17) | C9 | N3 | Zn1 | 100.2(2) |
| C13 | N3 | Zn1 | 115.48(17) | C10 | N3 | Zn1 | 112.0(2) |
| C6 | N2 | C8 | 122.7(2) | C11 | N3 | Zn1 | 107.3(3) |
| C8 | N2 | Zn1 | 115.86(19) | C9' | N3 | Zn1 | 104.0(2) |
| C9 | N3 | C13 | 109.5(2) | C11 | N3 | Zn1 | 112.3(2) |
| C1 | N1 | C5 | 118.7(3) | C12 | N4 | Zn1 | 162.3(2) |
| C10 | N3 | C13 | 107.5(2) | C13 | N5 | Zn1 | 175.5(2) |