Table 7.

¹H- and ¹³C-NMR data for compound 6 in C₅D₅N (500 MHz for ¹H and 125 MHz for ¹³C).

No.	δC	δH (J in Hz)	No.	δC	δH (J in Hz)
1	39.5	0.94 (m), 1.71 (m)	1'	103.6	4.93 (d, 7.5)
2	27.8	1.81 (m)	2'	80.2	4.39 (dd, 7.5, 8.5)
3	78.9	3.48 (dd, 5.0, 11.0)	3'	79.9	4.35 (dd, 8.5, 8.5)
4	40.2	—	4'	71.8	4.18 (m)
5	61.3	1.37 (d, 10.0)	5'	78.0	3.83 (m)
6	79.5	4.32 (m)	6'	62.9	4.31 (m)
7	45.0	1.93 (m), 2.35 (m)			4.57 (br. d, ca. 11)
8	41.2	—	1''	104.9	5.76 (d, 7.0)
9	50.0	1.48 (dd, 11.0, 11.0)	2''	75.9	4.16 (dd, 7.0, 8.5)
10	39.7	—	3''	78.8	4.25 (m)
11	30.9	1.50 (m), 2.04 (m)	4''	71.3	4.25 (m)
12	70.2	4.16 (m)	5''	67.3	3.66 (dd, 10.5, 10.5)
13	49.2	1.98 (dd, 10.5, 10.5)			4.33 (m)
14	51.4	—	1'''	98.1	5.11 (d, 7.0)
15	30.7	1.07 (m), 1.61 (m)	2'''	74.9	3.90 (dd, 7.0, 9.0)
16	26.6	1.28 (m), 1.72 (m)	3"'	79.3	4.17 (m)
17	51.6	2.51 (m)	4'''	71.6	4.05 (m)
18	17.59	1.15 (s)	5'''	77.1	4.06 (m)
19	17.55	0.97 (s)	6'''	70.3	4.31 (m)
20	83.5	—			4.72 (br. d, ca. 11)
21	22.3	1.63 (s) 3.63 (1H, m, overlapped)	1''''	105.4	5.09 (d, 7.5)
22	36.2	1.80 (m), 2.40 (m)	2''''	75.3	4.04 (m)
23	23.2	2.39 (m), 2.60 (m)	3"''	78.36	4.21 (m)
24	126.0	5.32 (t, 7.0)	4''''	71.7	4.21 (m)
25	131.1	—	5''''	78.41	3.92 (m)
26	25.8	1.61 (s)	6''''	62.8	4.36 (m)
27	18.0	1.67 (s)			4.51 (br. d, ca. 12)
28	31.7	2.06 (s)
29	16.7	1.46 (s)
30	17.2	0.80 (s)