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. 2013 Sep 2;18(9):10599–10608. doi: 10.3390/molecules180910599

Table 1.

1H-NMR (500 MHz) spectral data of xanthones 15.

Position Compound 1 1 Compound 2 2 Compound 3 2 Compound 4 2 Compound 5 2
1 13.72, s 13.42, s 13.44, s 13.72, s 13.79, s
4 6.28, s 6.24, s 6.30, s 6.26, s 6.37, s
5 6.80, s 6.74, s 6.75, s 6.85, s
11 3.35, d (J = 7.3 Hz) 3.37, d (J = 7.2 Hz) 3.36, d (J = 7.1 Hz) 6.74, d (J = 10.0 Hz) 3.48, d (J = 6.0 Hz)
12 5.17, t (J = 7.3 Hz) 5.17, t (J = 7.2 Hz) 5.26, t (J = 7.1 Hz) 5.58, d (J = 10.0 Hz) 5.31, t (J = 7.0 Hz)
14 1.77, s 1.75, s 1.70, s 1.27, s 1.79, s
15 1.63, s 1.62, s 1.71, s 1.28, s 1.71, s
16 4.04, d (J = 7.0 Hz) 4.09, d (J = 7.2 Hz) 4.15, d (J = 7.2, Hz) 4.10, d (J = 7.0 Hz) 3.59, d (J = 6.0 Hz)
17 5.17, t (J = 7.3 Hz) 5.18, t (J = 7.2 Hz) 5.26, t (J = 7.2 Hz) 5.27, t (J = 7.3 Hz) 5.31, t (J = 7.0 Hz)
19 1.71, s 1.61, s 1.70, s 1.71, s 1.87, s
20 1.73, s 1.72, s 1.82, s 1.82, s 1.89, s
3-OMe 3.82, s 3.91, s
6-OMe 3.97, s
7-OMe 3.71, s 3.80, s 3.82, s 3.83, s
1' 8.00, d (J = 10.0 Hz)
2' 5.79, d (J = 10.0 Hz)
4' 1.51, s
5' 1.51, s

1 DMSO-d6, 2 CDCl3.