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. 2013 Jun 14;18(6):6990–7003. doi: 10.3390/molecules18066990

Table 1.

The 1H-, 13C- and 15N-NMR coordination shifts (∆δ = δcomplexδligand; ppm) of the selected atoms and 195Pt chemical shifts (δ; ppm) of the prepared complexes.

1H-NMR 13C-NMR 15N-NMR 195Pt
C2H N6H C8H C2 C4 C5 C6 C8 N1 N3 N6 N7 N9
1 −0.09 0.82 0.84 1.35 −0.82 −4.07 −2.36 2.76 3.82 1.17 8.47 −105.03 5.60 −2077.10
2 0.18 0.52 0.84 1.41 −0.85 −4.03 −2.28 2.92 5.03 2.00 6.67 −105.02 6.17 −2072.08
3 0.17 0.60 0.88 1.37 −0.80 −4.01 −2.27 2.96 3.24 0.82 6.57 −106.00 4.96 −2074.81
4 0.19 0.51 0.92 1.27 −0.98 −4.14 −2.37 2.88 3.61 1.55 4.96 −106.69 5.45 −2071.38
5 0.12 0.69 0.72 1.61 −0.82 −3.90 −1.91 2.62 7.11 0.70 5.05 −105.70 5.09 −2076.80
6 0.18 0.59 0.84 1.31 −0.88 −4.07 −2.29 2.93 3.85 1.91 5.51 −105.78 6.21 −2074.68
7 0.15 0.75 0.69 1.49 −0.92 −3.97 −4.06 2.73 6.98 0.34 5.82 −106.22 4.78 −2078.30
8 0.19 0.52 0.90 1.31 −0.93 −4.13 −2.29 2.90 3.67 0.33 6.52 −105.37 6.32 −2071.68
9 0.19 0.55 0.83 1.34 −0.88 −4.07 −2.32 2.89 4.46 1.76 4.89 −106.10 5.86 −2073.15
10 0.26 0.83 −0.53 −1.19 −3.76 −0.66 3.03 3.13 −0.31 6.15 −106.52 5.02 −2084.94
11 0.60 0.83 1.30 −1.01 −3.68 −2.18 3.14 3.45 0.26 3.30 −106.24 5.00 −2083.47
12 0.81 0.69 1.34 −0.90 −3.66 −2.31 3.04 3.92 0.16 4.90 −105.72 5.03 −2088.28
13 0.85 0.78 0.12 −0.83 −3.27 −0.60 1.81 4.89 4.96 −105.76 5.33 −2091.62